Shapovalova I. Corrozio behaviour of constructional materials for the equipment of ozone synthesis of an oxygen containing derivatives of pyridine

Українська версія

Thesis for the degree of Candidate of Sciences (CSc)

State registration number

0407U004542

Thesis Registration Form

0407U004542.pdf

Applicant for

Specialization

  • 05.17.14 - Хімічний опір матеріалів та захист від корозії

07-11-2007

Specialized Academic Board

Д 26.002.13

Publishing and Printing Institute of Igor Sikorsky Kyiv Polytechnic Institute

Essay

The dissertation work contains results of complex experimental and theoretical study of influence of ozone, initial and finished of products on corrozion-electrochemical behaviour of constructional materials in processes ozone synthesis of pyridine N-оxide and of pyridinecarbon acids in neutral, acetic and sulfuric environments. The basic laws of corrosion of aluminium, carbonaceous , manganese containinq and some chromnickel steels in phosphatic рН 7 buffer, 5 % -s' acetic and 70% -s' sulfuric acid at presence of ozone, homologues of pyridine them N-оxides and of niacins are established. In conditions of industrial synthesis of a dipicolinic acid in a acetic solution, 4-methylpyridin-N-оxide in the phosphatic buffer, and also of preparatic synthesis of a niacin are carried out volt-ampere and of massmetric research of various constructional materials and the recommendations concerning their use for manufacturing of reactors of processes ozonization are submitted.

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Files

Автореферат_Шаповалової_І_М.doc

Дисертація Шаповалової І.М-Введение.doc

Дисертація Шаповалової І.М-Выводы.doc

Дисертація Шаповалової І.М-Литература.doc

Дисертація Шаповалової І.М-Раздел 1.doc

Дисертація Шаповалової І.М-Раздел 2.doc

Дисертація Шаповалової І.М-Раздел 3.doc

Дисертація Шаповалової І.М-Раздел 4.doc

Дисертація Шаповалової І.М-Раздел 5.doc

Дисертація Шаповалової І.М-Содержание.doc

Дисертація Шаповалової І.М-Титульный лист.doc

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